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Synthesis and crystal structure of a novel multimodal ligand, 6,6'-bis(2-(di(pyridin-2-yl)methylene)-1-methylhydrazinyl)-2,2'-bipyridine, and its copper(I) complex, {[Cu3L2](PF6)3° 3H2O} (1)
dipyridyl ketone metal complexes N-donor ligands
2010/12/3
The single crystal X-ray structure of the novel multimodal ligand 6,6'-bis(2-(di(pyridin-2-yl)methylene)-1-methylhydrazinyl)-2,2'-bipyridine, C34H28N10 (L), was determined at 120 (2) K. The ligand pos...
Synthesis and characterisations of some new 2,4-dihydro-[1,2,4]- triazol-3-one derivatives and X-ray crystal structures of 4-(3-phenylallylideneamino)-5-thiophen-2-yl-methyl-2,4-dihydro-[1,2,4]triazol-3-one
bromo acetophenone X-ray crystallography antimicrobial activity
2010/12/3
Compounds 2 were synthesised via the reaction of 4-amino-5-thiophen-2-yl-methyl-2,4-dihydro-[1,2,4]-triazol-3-one (1) with aldehydes. Compounds 3 and 4 were obtained from compounds 2 with bromo acetop...
Synthesis and crystal structure of a novel multimodal ligand, 6,6'-bis(2-(di(pyridin-2-yl)methylene)-1-methylhydrazinyl)-2,2'-bipyridine and its copper(I) complex, {[Cu3L2](PF6)3?3H2O} (1)
Bipyridine derivatives hydrazone dipyridyl ketone metal complexes
2010/10/19
The single crystal X-ray structure of the novel multimodal ligand 6,6’-bis(2-(di(pyridin-2-yl)methylene)-1-methylhydrazinyl)-2,2’-bipyridine, C34H28N10 (L), was determined at 120 (2) K. The ligand pos...
Synthesis and Characterizations of Some New 2,4-Dihydro-[1,2,4]-triazol-3-one Derivatives and X-Ray Crystal Structures of 4-(3-Phenyl allidene amino)-5-thiophen-2-yl-methyl-2,4-dihydro-[1,2,4]triazol-3-one
1,2,4-Triazole aldehydes ethyl bromoacetate bromo acetophenone
2010/10/19
Compounds 2 were synthesised via the reaction of 4-amino-5-thiophen-2-yl-methyl-2,4-dihydro-[1,2,4]-triazol-3-one (1) with aldehydes. Compounds 3 and 4 were obtained from compounds 2 with bromo acetop...
Synthesis, Spectroscopic Characterization, Mass Spectrometry and Crystal Structure of N-{[(4-bromophenyl) amino]carbonothioyl}benzamide
Thiourea derivative X-ray structure determination mass fragmentation
2010/10/19
N-{[(4-bromophenyl)amino]carbonothioyl}benzamide was synthesized and characterized by IR, 1 H- and 13C-NMR, mass spectrometry, and elemental analysis. The crystal structure was determined from single ...
Synthesis, characterization, crystal structures, and antibacterial activity of some new 1-(3,4,5-trimethoxybenzoyl)-3-aryl thioureasreas
1-(3,4,5-trimethoxy)benzoyl-3-arylthioureas antibacterial crystal structure
2010/10/18
Synthesis of some novel 1-(3,4,5-trimethoxy)benzoyl-3- arylthiourea derivatives (1a-o) was accomplished in 2 steps. The synthetic route involves the reaction of 1-(3,4,5-trimethoxy)benzoyl chloride wi...
The Effect of Electrocatalytic Activity and Crystal Structure of PbO2 Surfaces on Polyphenylene Oxide (PPO) Production in Acetonitrile
a-PbO2 b -PbO2 phenol electrocatalysis PPO
2010/4/9
The crystallographic nature of PbO2 films was changed by optimizing the electrolysis conditions in an electrodeposition solution of PbO2. These PbO2 films were then used to prepare PPO films. It was d...
The Effect of Electrocatalytic Activity and Crystal Structure of PbO2 Surfaces on Polyphenylene Oxide (PPO) Production in Acetonitrile
a-PbO2 b -PbO2 phenol electrocatalysis PPO
2010/4/9
The crystallographic nature of PbO2 films was changed by optimizing the electrolysis conditions in an electrodeposition solution of PbO2. These PbO2 films were then used to prepare PPO films. It was d...
The Crystal Structure of 2-Nitro-N-(4-nitrophenyl)benzamide
X-ray structure 2-nitro-N-(4-nitrophenyl)benzamide
2010/4/16
2-Nitro-N-(4-nitrophenyl)benzamide was synthesized and characterized by spectroscopy and elemental analysis. The crystal structure was determined from single-crystal X-ray diffraction data. It crystal...
Dinuclear Molybdenum Tetracarbonyl Complexes of Tetradentate Nitrogen Ligands and Intermolecular Hydrogen Bonding in the Crystal Structure of N,N´-bis-[1-(pyridin-2-yl)ethylidene]-ethane-1,2-diamine
Dinuclear intermolecular H-bonding molybdenum polyimines Schiff base tetracarbonyl
2010/4/8
Multidentate N-ligands (Schiff bases) were prepared by the condensation of 2-acetylpyridine or 2-benzoylpyridine, and 1,2-diaminoethane or 1,6-diaminohexane (2:1 ratio) in ethanol. These ligands were ...
The Mechanism and Crystal Structure of 2-Methoxy-2-methyl-4-phenyl-3,4,4a, 10b-tetrahydro-2H,5H-pyrano[3,2-c]chromen-5-one. Acetal of Warfarin Acid
Warfarin acid synthesis acetal crystal structure
2010/4/19
Acetal of warfarin acid has been synthesized via a hemi acetal intermediate and structurally characterized by X-ray diffraction. The crystal structure shows that the title compound was formed by the h...
Synthesis, Crystal Structure and Antifungal/Antibacterial Activity of Some Novel Highly Functionalized Benzoylaminocarbothioyl Pyrrolidines
Pyrrolidine derivatives aminocarbothioyl derivatives bioactivity antibacterial activity antifungal activity toxicity
2010/4/19
A series of novel highly functionalized benzoylaminocarbothioyl pyrrolidines were prepared from benzoylisothiocyanate and substituted pyrrolidines in excellent yield. The crystal structure of the nove...
Synthesis and Crystal Structure of 1,3-Bis(5-formylpyrrol-2-yl)benzene and Its Conversion to a Macrocyclic Derivative
Schiff Base Bisformylpyrrole Macrocycle Crystal structure
2010/4/19
This report details the synthesis and characterization of a new diformyl pyrrole derivative 2 and its macrocyclic derivative 3. The new compounds were characterized by FT-IR, 13C NMR, and 1H NMR spect...
The Crystal and Molecular Structure of New Hydrogen Dinitrate of Nitrato(2,2',2''-terpyridyl)platinum(II) Ion, [Pt(terpy)ONO2][H(ONO2)2]
X-ray structure terpyridine hydrogen nitrate platinum complex
2010/4/20
The title compound, C15H12N6O9Pt, consists of [Pt(terpy)ONO2]+ cation and [H(ONO2)2]- anion, in which 2 nitrate groups are linked by a strong hydrogen bond [O \cdots O 2449(1) Å]. In the cation,...
Crystal Structure of the cis-bis[4-chloro-N-(pyrrolidine-1-carbothioyl)-benzamido] copper(II) Complex
Thioureas X-ray structures Benzoylthiourea complexes Cu(II) complex
2010/4/20
The crystal and molecular structure of the cis-bis[4-chloro-N-(pyrrolidine-1-carbothioyl)-benzamido] copper(II) complex was determined by single-crystal X-ray diffraction. The title compound, C24H24N4...