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A Mild Method for the Cleavage of Ketals Using IBX
Deprotection ketal IBX ketone single electron transfer batrachotoxin
2010/4/9
Investigation on the total synthesis of batrachotoxin 1 revealed that the cyclic ketals could be cleaved to ketone with IBX in DMSO at 70-81 °C under very mild conditions. A variety of functional grou...